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N, N-bis(2-chloroethyl)-N-methyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl] methanaminium bromide

Base Information Edit
  • Chemical Name:N, N-bis(2-chloroethyl)-N-methyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl] methanaminium bromide
  • CAS No.:1346936-27-3
  • Molecular Formula:Br*C18H29BCl2NO2
  • Molecular Weight:453.055
  • Hs Code.:
  • Mol file:1346936-27-3.mol
N, N-bis(2-chloroethyl)-N-methyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl] methanaminium bromide

Synonyms:N, N-bis(2-chloroethyl)-N-methyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl] methanaminium bromide

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Chemical Property of N, N-bis(2-chloroethyl)-N-methyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl] methanaminium bromide Edit
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Technology Process of N, N-bis(2-chloroethyl)-N-methyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl] methanaminium bromide

There total 3 articles about N, N-bis(2-chloroethyl)-N-methyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl] methanaminium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
mechlorethamine hydrochloride; With potassium hydroxide; for 0.0833333h; Cooling with ice;
4-bromomethylphenylboronic acid pinacol ester; In dichloromethane; at 20 ℃; for 72h;
Guidance literature:
Multi-step reaction with 3 steps
1: thionyl chloride / 20 °C
2: dihydrogen peroxide / water-d2 / 2 h / pH 7.5 / aq. phosphate buffer
3: dichloromethane / 72 h / 20 °C
With thionyl chloride; dihydrogen peroxide; In dichloromethane; water-d2;
DOI:10.1021/ja2073824
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