Technology Process of C30H15BrF17NO6S
There total 8 articles about C30H15BrF17NO6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Ti2CO3;
tetrakis(triphenylphosphine) palladium(0);
In
benzene;
at 80 ℃;
for 24h;
DOI:10.1039/b516487g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: KOH / dimethylformamide / 0.17 h
1.2: iodine / dimethylformamide / 0.5 h
2.1: 88 percent / Et3N; DMAP / CH2Cl2 / 12 h / 20 °C
3.1: 88 percent / Et3N / PdCl2(dppf)2*CH2Cl2 (1:1) / dioxane / 4 h / 80 °C
4.1: 100 percent / Tl2CO3 / Pd(PPh3)4 / benzene / 24 h / 80 °C
With
dmap; potassium hydroxide; Ti2CO3; triethylamine;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1039/b516487g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 88 percent / Et3N; DMAP / CH2Cl2 / 12 h / 20 °C
2: 88 percent / Et3N / PdCl2(dppf)2*CH2Cl2 (1:1) / dioxane / 4 h / 80 °C
3: 100 percent / Tl2CO3 / Pd(PPh3)4 / benzene / 24 h / 80 °C
With
dmap; Ti2CO3; triethylamine;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; dichloromethane; benzene;
DOI:10.1039/b516487g