3-chlorobenzalchloroimine

Base Information

• Chemical Name: 3-chlorobenzalchloroimine
• CAS No.: 860554-30-9
• Molecular Formula: C₇H₅Cl₂N
• Molecular Weight: 174.029
• Mol file: 860554-30-9.mol

Synonyms:3-chlorobenzalchloroimine

Chemical Property of 3-chlorobenzalchloroimine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 3-chlorobenzalchloroimine

There total 4 articles about 3-chlorobenzalchloroimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Chloro-benzylideneamine → 3-chlorobenzalchloroimine (860554-30-9)

Guidance literature:

With sodium chlorite; In ethanol; at 50 ℃; for 2h;

DOI:10.3184/174751918X15403084696731

Reference yield:

m-Chlorobenzaldehyde (587-04-2) → 3-chlorobenzalchloroimine (860554-30-9)

Guidance literature:

With chloroamine; diethyl ether; at 0 ℃;

DOI:10.1021/ja01306a054

Reference yield:

C7H6Cl3N → 3-chlorobenzalchloroimine (860554-30-9)

Guidance literature:

With triethylamine; at 20 ℃; for 0.166667h; Milling;

DOI:10.1002/ejoc.201700689

upstream raw materials:

m-Chlorobenzaldehyde

m-chlorobenzylamine

Downstream raw materials:

3-chloro-benzonitrile

m-Chlorobenzaldehyde

Refernces

• 1、 Gaspa, Silvia,Porcheddu, Andrea,Valentoni, Antonio,Garroni, Sebastiano,Enzo, Stefano,De Luca, Lidia. "A Mechanochemical-Assisted Oxidation of Amines to Carbonyl Compounds and Nitriles". . p. 5519 - 5526. Retrieved 2017/09/06.