di-tert-butyl 2,2'-(benzylimino)diacetate

Base Information

• Chemical Name: di-tert-butyl 2,2'-(benzylimino)diacetate
• CAS No.: 275371-57-8
• Molecular Formula: C₁₉H₂₉NO₄
• Molecular Weight: 335.444
• Mol file: 275371-57-8.mol

Synonyms:di-tert-butyl 2,2'-(benzylimino)diacetate

Chemical Property of di-tert-butyl 2,2'-(benzylimino)diacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of di-tert-butyl 2,2'-(benzylimino)diacetate

There total 2 articles about di-tert-butyl 2,2'-(benzylimino)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

bromoacetic acid tert-butyl ester (5292-43-3) + benzylamine (100-46-9) → di-tert-butyl 2,2'-(benzylimino)diacetate (275371-57-8)

Guidance literature:

With potassium carbonate; In acetonitrile; at 25 ℃; for 12h; sonication;

DOI:10.1021/jo026833k

Reference yield:

→ di-tert-butyl 2,2'-(benzylimino)diacetate (275371-57-8)

Guidance literature:

Reference yield: 98.0%

di-tert-butyl 2,2'-(benzylimino)diacetate (275371-57-8) → tert-butyl iminodiacetate (85916-13-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; at 25 ℃; for 20h;

DOI:10.1021/jo026833k

upstream raw materials:

bromoacetic acid tert-butyl ester

benzylamine

Downstream raw materials:

tert-butyl iminodiacetate

Refernces

• 1、 Roy, Bidhan C.,Santos, Marina,Mallik, Sanku,Campiglia, Andres D.. "Synthesis of metal-chelating lipids to sensitize lanthanide ions". . p. 3999 - 4007. Retrieved 2007/10/03.