Perfluorosebacamidine

Base Information

• Chemical Name: Perfluorosebacamidine
• CAS No.: 865-94-1
• Molecular Formula: C₁₀H₆F₁₆N₄
• Molecular Weight: 486.159
• Hs Code.: 2925290090
• DSSTox Substance ID: DTXSID40380015
• Wikidata: Q82170040
• Mol file: 865-94-1.mol

Synonyms:Perfluorosebacamidine;865-94-1;2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecanediimidamide;C10H6F16N4;SCHEMBL322433;DTXSID40380015;XHXXTJKMMCVPCP-UHFFFAOYSA-N;MFCD00054684;AKOS015852402;FS-6058;FT-0676900;A841736;2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecanebis(imidamide);2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecakis(fluoranyl)decanediimidamide

Chemical Property of Perfluorosebacamidine

Chemical Property:

• Vapor Pressure: 0.017mmHg at 25°C
• Melting Point: 175-178 °C
• Refractive Index: 1.352
• Boiling Point: 254.7°C at 760 mmHg
• PKA: 6.68±0.40(Predicted)
• Flash Point: 107.8°C
• PSA: 99.74000
• Density: 1.8g/cm³
• LogP: 5.54080
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 18
• Rotatable Bond Count: 9
• Exact Mass: 486.0336968
• Heavy Atom Count: 30
• Complexity: 651

Purity/Quality:

98%Min ^*data from raw suppliers

Perfluorosebacamidine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(=N)(C(C(C(C(C(C(C(C(C(=N)N)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)N

Technology Process of Perfluorosebacamidine

There total 4 articles about Perfluorosebacamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.4%

perfluorosebaconitrile (2342-09-8,25302-65-2) → perfluorosebacodiamidine (865-94-1)

Guidance literature:

With ammonia; at -28 ℃; for 1h;

DOI:10.1016/S0022-1139(00)81467-0

Reference yield:

Perfluordodecan-1,12-dicarbonsaeure (2822-93-7) → perfluorosebacodiamidine (865-94-1)

Guidance literature:

Multi-step reaction with 4 steps

1: FSO₃H

2: NH₃ / diethyl ether

3: P₂O₅

4: liq. NH₃

With ammonia; fluorosulphonic acid; phosphorus pentoxide; In diethyl ether;

DOI:10.1007/BF00846975

Reference yield:

Perfluordodecan-1,12-dicarbonsaeure-diethylester (3799-53-9) → perfluorosebacodiamidine (865-94-1)

Guidance literature:

Multi-step reaction with 3 steps

1: NH₃ / diethyl ether

2: P₂O₅

3: liq. NH₃

With ammonia; phosphorus pentoxide; In diethyl ether;

DOI:10.1007/BF00846975

upstream raw materials:

perfluorosebaconitrile

Perfluordodecan-1,12-dicarbonsaeure

Perfluordodecan-1,12-dicarbonsaeure-diethylester

perfluorosebacic acid diamide

Refernces