2-hydroxy-4,6-dimethoxyacetophenone monoacetate

Base Information Edit

Chemical Name:2-hydroxy-4,6-dimethoxyacetophenone monoacetate
CAS No.:59263-72-8
Molecular Formula:C₁₂H₁₄O₅
Molecular Weight:238.24
Hs Code.:
Mol file:59263-72-8.mol

Synonyms:2-hydroxy-4,6-dimethoxyacetophenone monoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-4,6-dimethoxyacetophenone monoacetate Edit

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Technology Process of 2-hydroxy-4,6-dimethoxyacetophenone monoacetate

There total 4 articles about 2-hydroxy-4,6-dimethoxyacetophenone monoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 90-24-4
2-hydroxy-4,6-dimethoxyacetophenone

: 108-24-7
acetic anhydride

: 59263-72-8
2-hydroxy-4,6-dimethoxyacetophenone monoacetate

Guidance literature:: In pyridine; for 0.0833333h; Heating;
DOI:10.1002/jps.2600840416

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 59263-72-8
2-hydroxy-4,6-dimethoxyacetophenone monoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: ZnCl₂; diethyl ether; HCl / und Erhitzen des Reaktionsprodukts mit Wasser

2: sodium acetate

With hydrogenchloride; diethyl ether; sodium acetate; zinc(II) chloride;