(+)-(2S,4R)-trans-2,4-dimethyl-1-cyclohexanone

Base Information Edit

Chemical Name:(+)-(2S,4R)-trans-2,4-dimethyl-1-cyclohexanone
CAS No.:93921-42-7
Molecular Formula:C₈H₁₄O
Molecular Weight:126.199
Hs Code.:
Mol file:93921-42-7.mol

Synonyms:(+)-(2S,4R)-trans-2,4-dimethyl-1-cyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(2S,4R)-trans-2,4-dimethyl-1-cyclohexanone Edit

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Technology Process of (+)-(2S,4R)-trans-2,4-dimethyl-1-cyclohexanone

There total 22 articles about (+)-(2S,4R)-trans-2,4-dimethyl-1-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 111003-03-3
c-2,t-4-Dimethyl-r-1-cyclohexanol

: 93921-42-7
(+)-(2S,4R)-trans-2,4-dimethyl-1-cyclohexanone

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 1.5h;

Reference yield:

: 105-67-9
2,4-Xylenol

: 823-55-2,4888-64-6,6258-29-3,69256-18-4,82467-29-6,82467-30-9,93921-42-7,111003-06-6,116783-29-0
cis-2,4-dimethylcyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / W₄ Raney Ni / ethanol / 160 - 170 °C / 106400 Torr

2: sodium acetate / 1.) 140 deg C, 4 h , 2.) Bacillus subtilis var. niger IFO 3108, H₂O, 27 deg C, 2 d

3: CrO₃, conc. H₂SO₄ / acetone; H₂O

With chromium(VI) oxide; sulfuric acid; hydrogen; sodium acetate; W₄ Raney Ni; In ethanol; water; acetone;

Reference yield:

: 23713-65-7,59338-76-0,59338-77-1,59338-78-2,82416-23-7,82416-24-8,82416-25-9,82416-26-0,82416-31-7,82416-32-8,111003-03-3,111003-05-5,113776-10-6,69542-91-2
2,4-dimethylcyclohexan-1-ol

: 823-55-2,4888-64-6,6258-29-3,69256-18-4,82467-29-6,82467-30-9,93921-42-7,111003-06-6,116783-29-0
cis-2,4-dimethylcyclohexanone

: 823-55-2,4888-64-6,6258-29-3,69256-18-4,82467-29-6,82467-30-9,93921-42-7,111003-06-6,116783-29-0
trans-2,4-dimethylcyclohexanone

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In water; acetone; Yield given. Yields of byproduct given. Title compound not separated from byproducts;