2-(carboxymethoxy)-3-methylbenzoic acid

Base Information Edit

Chemical Name:2-(carboxymethoxy)-3-methylbenzoic acid
CAS No.:60770-15-2
Molecular Formula:C₁₀H₁₀O₅
Molecular Weight:210.186
Hs Code.:
Mol file:60770-15-2.mol

Synonyms:2-(carboxymethoxy)-3-methylbenzoic acid

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Chemical Property of 2-(carboxymethoxy)-3-methylbenzoic acid Edit

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Technology Process of 2-(carboxymethoxy)-3-methylbenzoic acid

There total 6 articles about 2-(carboxymethoxy)-3-methylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1616110-77-0
methyl 2-(2-ethoxy-2-oxoethoxy)-3-methylbenzoate

: 60770-15-2
2-(carboxymethoxy)-3-methylbenzoic acid

Guidance literature:: With potassium hydroxide; In methanol; water; Reflux;
DOI:10.1021/acs.jmedchem.8b01709

Reference yield:

: 23287-26-5
3-methylsalicylic acid methyl ester

: 105-36-2
ethyl bromoacetate

: 60770-15-2
2-(carboxymethoxy)-3-methylbenzoic acid

Guidance literature:: With methanol; sodium methylate; anschliessende Hydrolyse;
DOI:10.1021/ja01642a026

Reference yield:

: 83-40-9
3-methylsalicylic acid

: 60770-15-2
2-(carboxymethoxy)-3-methylbenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 12 h / Reflux

2.1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 12 h / 20 °C

3.1: potassium hydroxide / methanol / 4 h / Reflux

3.2: 0 °C / pH 1

With thionyl chloride; potassium carbonate; sodium iodide; potassium hydroxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm5002502