C₂₄H₃₉N₃O₃

Base Information

• Chemical Name: C₂₄H₃₉N₃O₃
• CAS No.: 1228432-56-1
• Molecular Formula: C₂₄H₃₉N₃O₃
• Molecular Weight: 417.592
• Mol file: 1228432-56-1.mol

Synonyms:C₂₄H₃₉N₃O₃

Chemical Property of C₂₄H₃₉N₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₃₉N₃O₃

There total 1 articles about C₂₄H₃₉N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

L-leucyl-L-leucine methyl ester (13022-42-9,77167-62-5,84728-06-3,97187-65-0) + [1'(R)-α-methylbenzyl]aziridine-2(R)-carboxaldehyde → C24H39N3O3 (1228432-56-1)

Guidance literature:

L-leucyl-L-leucine methyl ester; [1'(R)-α-methylbenzyl]aziridine-2(R)-carboxaldehyde; With magnesium sulfate; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

With sodium cyanoborohydride; In methanol; at 20 ℃;

DOI:10.5012/bkcs.2010.31.03.611

Reference yield: 84.5%

bis(trichloromethyl) carbonate (32315-10-9) + C24H39N3O3 (1228432-56-1) → C25H38ClN3O4 (1228432-57-2)

Guidance literature:

C₂₄H₃₉N₃O₃; With sodium hydride; In tetrahydrofuran; at -10 ℃; for 1h;

bis(trichloromethyl) carbonate; In tetrahydrofuran; for 2h;

DOI:10.5012/bkcs.2010.31.03.611

upstream raw materials:

L-leucyl-L-leucine methyl ester

Downstream raw materials:

C₂₅H₃₈ClN₃O₄

Refernces