Technology Process of bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III)
There total 5 articles about bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium carbonate; hydrazine hydrate / ethanol / 12 h / Inert atmosphere; Cooling with ice
2.1: sodium carbonate / tetrahydrofuran; N,N-dimethyl acetamide / 0.25 h / 0 °C / Inert atmosphere
2.2: 15 h / Inert atmosphere
3.1: sodium carbonate / 2-ethoxy-ethanol / 20 h / 130 °C / Inert atmosphere
With
sodium carbonate; hydrazine hydrate;
In
tetrahydrofuran; 2-ethoxy-ethanol; ethanol; N,N-dimethyl acetamide;
DOI:10.1016/j.dyepig.2016.03.006
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium carbonate / tetrahydrofuran; N,N-dimethyl acetamide / 0.25 h / 0 °C / Inert atmosphere
1.2: 15 h / Inert atmosphere
2.1: sodium carbonate / 2-ethoxy-ethanol / 20 h / 130 °C / Inert atmosphere
With
sodium carbonate;
In
tetrahydrofuran; 2-ethoxy-ethanol; N,N-dimethyl acetamide;
DOI:10.1016/j.dyepig.2016.03.006