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(R)-(+)-1,9-fluorenylethylchloroformate

Base Information Edit
  • Chemical Name:(R)-(+)-1,9-fluorenylethylchloroformate
  • CAS No.:1428936-75-7
  • Molecular Formula:C16H13ClO2
  • Molecular Weight:272.731
  • Hs Code.:
  • Mol file:1428936-75-7.mol
(R)-(+)-1,9-fluorenylethylchloroformate

Synonyms:(R)-(+)-1,9-fluorenylethylchloroformate

Suppliers and Price of (R)-(+)-1,9-fluorenylethylchloroformate
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
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  • Chemicals and raw materials
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Total 4 raw suppliers
Chemical Property of (R)-(+)-1,9-fluorenylethylchloroformate Edit
Chemical Property:
Purity/Quality:

99% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
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Technology Process of (R)-(+)-1,9-fluorenylethylchloroformate

There total 3 articles about (R)-(+)-1,9-fluorenylethylchloroformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: (S)-diphenylprolinol / tert-butyl methyl ether / 0.75 h / 45 °C
2: pyridine; triethylamine / dichloromethane / 2 h / 0 - 25 °C
With pyridine; (S)-diphenylprolinol; triethylamine; In dichloromethane; tert-butyl methyl ether; 1: |Corey-Bakshi-Shibata Reduction;
DOI:10.1039/c3ob40218e
Guidance literature:
Multi-step reaction with 3 steps
1: potassium tert-butylate / diethyl ether / 7.5 h / Inert atmosphere; Reflux
2: (S)-diphenylprolinol / tert-butyl methyl ether / 0.75 h / 45 °C
3: pyridine; triethylamine / dichloromethane / 2 h / 0 - 25 °C
With pyridine; (S)-diphenylprolinol; potassium tert-butylate; triethylamine; In diethyl ether; dichloromethane; tert-butyl methyl ether; 2: |Corey-Bakshi-Shibata Reduction;
DOI:10.1039/c3ob40218e
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