Technology Process of bis(3,5-di-tert-butyl-4-(hydrogenphenylboronoxy)phenyl)methane
There total 1 articles about bis(3,5-di-tert-butyl-4-(hydrogenphenylboronoxy)phenyl)methane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
n-butyllithium;
In
hexane; toluene;
byproducts: LiCl; n-C4H9Li in hexane was added dropwise to a soln. of phenol-compound in toluene in N2 atm., the mixt. was heated at 100°C overnight, cooled to room temp., Cl2BC6H5 was added, heated for 12 h; ppt. was dissolved washing with water, dried over MgSO4, the solvent wasremoved in vac.; elem. anal.;
DOI:10.1021/ic800204q