BUTETH-3 CARBOXYLIC ACID

Base Information

• Chemical Name: BUTETH-3 CARBOXYLIC ACID
• CAS No.: 75427-76-8
• Molecular Formula: C10H20 O5
• Molecular Weight: 220.26
• Mol file: 75427-76-8.mol

Synonyms:Aceticacid, [2-(2-butoxyethoxy)ethoxy]- (9CI)

Chemical Property of BUTETH-3 CARBOXYLIC ACID

Chemical Property:

• Boiling Point: 138 - 150 °C (0.3 mmHg)
• PSA: 64.99000
• LogP: 0.92090

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BUTETH-3 CARBOXYLIC ACID

There total 4 articles about BUTETH-3 CARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

triethyleneglycol monobutyl ether (143-22-6,9004-77-7) → 3,6,9-trioxatridecanoic acid (75427-76-8,107600-34-0)

Guidance literature:

With potassium hydroxide; potassium permanganate; In water; for 12h; Ambient temperature;

Reference yield: 55.0%

Diethylene glycol monobutyl ether (112-34-5,9004-77-7) + chloroacetic acid (79-11-8) → 3,6,9-trioxatridecanoic acid (75427-76-8,107600-34-0)

Guidance literature:

With sodium hydride; In tetrahydrofuran; Inert atmosphere;

DOI:10.1016/j.ejmech.2020.112408

Reference yield:

Diethylene glycol monobutyl ether (112-34-5,9004-77-7) → 3,6,9-trioxatridecanoic acid (75427-76-8,107600-34-0)

Guidance literature:

With sodium hydroxide; at 50 ℃; Behandeln des Reaktionsprodukts mit Chloressigsaeure;

upstream raw materials:

Diethylene glycol monobutyl ether

triethyleneglycol monobutyl ether

chloroacetic acid

Downstream raw materials:

3-Benzyloxypropylenbis(3,6,9-trioxatridecanoat)

Refernces

• 1、 Craine,Greenblatt,Woodson,Hortelano,Raban. "CONFIGURATIONAL BIASING OF TERTIARY AMIDE IONOPHORES BY ALKALI METAL CHELATION1,2.". . p. 7252 - 7255. Retrieved 2007/10/02.