1,2-dibromo-1-cyclohexylethane

Base Information

• Chemical Name: 1,2-dibromo-1-cyclohexylethane
• CAS No.: 81602-60-0
• Molecular Formula: C₈H₁₄Br₂
• Molecular Weight: 270.007
• Mol file: 81602-60-0.mol

Synonyms:1,2-dibromo-1-cyclohexylethane

Chemical Property of 1,2-dibromo-1-cyclohexylethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-dibromo-1-cyclohexylethane

There total 1 articles about 1,2-dibromo-1-cyclohexylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

vinylcyclohexane (695-12-5,25498-06-0) → 1,2-dibromo-1-cyclohexylethane (81602-60-0)

Guidance literature:

With bromine; In chloroform; at 0 - 20 ℃; for 1h; Inert atmosphere;

DOI:10.1055/s-0037-1611228

Reference yield: 88.0%

1,2-dibromo-1-cyclohexylethane (81602-60-0) → 1-bromo-1-cyclohexylethylene (85970-80-5)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1055/s-0037-1611228

Reference yield: 52.0%

1,2-dibromo-1-cyclohexylethane (81602-60-0) → 2-cyclohexylacetylene (931-48-6)

Guidance literature:

With sodium hydroxide; PEG 600 ; at 80 ℃; for 5h;

DOI:10.1021/jo00133a056

upstream raw materials:

vinylcyclohexane

Downstream raw materials:

2-cyclohexylacetylene

1-bromo-1-cyclohexylethylene

trans-1-methoxy-4-(2-cyclohexylethenyl)benzene

cis,cis-Dicyclohexyl-buta-1,3-dien

Refernces

• 1、 Alom, Nur-E,Wu, Fan,Li, Wei. "One-Pot Strategy for Thiazoline Synthesis from Alkenes and Thioamides". supporting information. p. 930 - 933. Retrieved 2017/02/26.