Trichlormethansulfinsaeureanilid

Base Information

• Chemical Name: Trichlormethansulfinsaeureanilid
• CAS No.: 42521-52-8
• Molecular Formula: C₇H₆Cl₃NOS
• Molecular Weight: 258.556
• Mol file: 42521-52-8.mol

Synonyms:Trichlormethansulfinsaeureanilid

Chemical Property of Trichlormethansulfinsaeureanilid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Trichlormethansulfinsaeureanilid

There total 3 articles about Trichlormethansulfinsaeureanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trichloro-methanesulfenic acid anilide (16188-39-9) → Trichlormethansulfinsaeureanilid (42521-52-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; Yield given;

DOI:10.1016/S0040-4039(96)02351-9

Reference yield:

aniline (62-53-3) → Trichlormethansulfinsaeureanilid (42521-52-8)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / 0 °C

2: MCPBA / CH₂Cl₂ / 0 °C

With 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;

DOI:10.1016/S0040-4039(96)02351-9

Reference yield:

trichloromethanesulfinyl chloride (25004-95-9) + aniline (62-53-3) → Trichlormethansulfinsaeureanilid (42521-52-8)

Guidance literature:

upstream raw materials:

trichloromethanesulfinyl chloride

aniline

trichloro-methanesulfenic acid anilide

Downstream raw materials:

chloroform

N-phenylsulfinylamine

Refernces