dimethyl 4,4′-(carbonylbis(oxy))dibenzoate

Base Information

• Chemical Name: dimethyl 4,4′-(carbonylbis(oxy))dibenzoate
• CAS No.: 74721-70-3
• Molecular Formula: C₁₇H₁₄O₇
• Molecular Weight: 330.294
• Mol file: 74721-70-3.mol

Synonyms:dimethyl 4,4′-(carbonylbis(oxy))dibenzoate

Chemical Property of dimethyl 4,4′-(carbonylbis(oxy))dibenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of dimethyl 4,4′-(carbonylbis(oxy))dibenzoate

There total 4 articles about dimethyl 4,4′-(carbonylbis(oxy))dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

bis(trichloromethyl) carbonate (32315-10-9) + methyl 4-hydroxylbenzoate (99-76-3,156291-94-0) → dimethyl 4,4′-(carbonylbis(oxy))dibenzoate (74721-70-3)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃; for 16h;

DOI:10.1039/c5ob02240a

Reference yield:

methyl 4-hydroxylbenzoate (99-76-3,156291-94-0) → dimethyl 4,4′-(carbonylbis(oxy))dibenzoate (74721-70-3)

Guidance literature:

Multi-step reaction with 2 steps

1: quinoline; benzene

2: benzene

With quinoline; benzene;

Reference yield:

phosgene (75-44-5) + methyl 4-hydroxylbenzoate (99-76-3,156291-94-0) → dimethyl 4,4′-(carbonylbis(oxy))dibenzoate (74721-70-3)

Guidance literature:

With sodium hydroxide;

upstream raw materials:

phosgene

methyl 4-hydroxylbenzoate

methyl 4-[(chlorocarbonyl)oxy]benzoate

2-(Diethylamino)ethanol

Downstream raw materials:

carbon dioxide

dimethyl 4,4'-oxydibenzoate

methyl 4-((dimethylcarbamoyl)oxy)benzoate

Refernces