Technology Process of fac-(N-benzoyl-4-(aminomethyl)pyridine)(2,2'-bipyridine)(CO)3Re(I)(1+)
There total 1 articles about fac-(N-benzoyl-4-(aminomethyl)pyridine)(2,2'-bipyridine)(CO)3Re(I)(1+) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
silver(I) hexafluorophosphate;
In
N,N-dimethyl-formamide;
byproducts: AgCl; heating of soln. of educts to 70°C, react. time 30-40 min, TLC monoitoring (silica gel, MeOH-CH2Cl2) of react.; cooling soln., evapn. of DMF, dissoluting of product in CH2Cl2, removing solid AgCl by filtn., evapn. of CH2Cl2, chromy. on silica gel (MeOH-CH2Cl2);