Technology Process of C20H30N4O
There total 7 articles about C20H30N4O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium; propan-1-ol / toluene / 12 h / Reflux; Inert atmosphere
2: tetrahydrofuran / 72 h / 20 °C / Inert atmosphere
3: hydrogenchloride / methanol; 1,4-dioxane / 2 h / 20 °C / Inert atmosphere
4: sodium carbonate / water; dichloromethane / 0 - 20 °C / Inert atmosphere
5: phosphorus pentachloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
6: dichloromethane; tert-Amyl alcohol / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; propan-1-ol; phosphorus pentachloride; sodium; sodium carbonate;
In
tetrahydrofuran; 1,4-dioxane; methanol; tert-Amyl alcohol; dichloromethane; water; toluene;
DOI:10.1021/ml400370w
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride / methanol; 1,4-dioxane / 2 h / 20 °C / Inert atmosphere
2: sodium carbonate / water; dichloromethane / 0 - 20 °C / Inert atmosphere
3: phosphorus pentachloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
4: dichloromethane; tert-Amyl alcohol / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; phosphorus pentachloride; sodium carbonate;
In
1,4-dioxane; methanol; tert-Amyl alcohol; dichloromethane; water;
DOI:10.1021/ml400370w
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrahydrofuran / 72 h / 20 °C / Inert atmosphere
2: hydrogenchloride / methanol; 1,4-dioxane / 2 h / 20 °C / Inert atmosphere
3: sodium carbonate / water; dichloromethane / 0 - 20 °C / Inert atmosphere
4: phosphorus pentachloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
5: dichloromethane; tert-Amyl alcohol / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; phosphorus pentachloride; sodium carbonate;
In
tetrahydrofuran; 1,4-dioxane; methanol; tert-Amyl alcohol; dichloromethane; water;
DOI:10.1021/ml400370w