DIHYDROSORBICILLIN

Base Information

• Chemical Name: DIHYDROSORBICILLIN
• CAS No.: 79950-82-6
• Molecular Formula: C14H18 O3
• Molecular Weight: 234.295
• Mol file: 79950-82-6.mol

Synonyms:4-Hexen-1-one,1-(2,4-dihydroxy-3,5-dimethylphenyl)-, (E)-; 2',3'-Dihydrosorbicillin

Chemical Property of DIHYDROSORBICILLIN

Chemical Property:

• PSA: 57.53000
• LogP: 3.25360

Purity/Quality:

DIHYDROSORBICILLIN 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIHYDROSORBICILLIN

There total 7 articles about DIHYDROSORBICILLIN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

1-<(4R*,5S*)-4,5-dibromohexanoyl>-2,4-dihydroxy-3,5-dimethylbenzene → 2',3'-dihydrosorbicillin (79950-82-6)

Guidance literature:

With zinc; In diethyl ether; acetic acid; for 2h; Ambient temperature;

DOI:10.1016/S0040-4020(01)88647-6

Reference yield: 14.0%

sorbicillin (79950-85-9) → 2',3'-dihydrosorbicillin (79950-82-6) + 2,4-dimethyl-6-hexanoyl-resorcinol (88924-67-8) + 2',5'-dihydrosorbicillin (88924-68-9)

Guidance literature:

With hydrogen; platinum(IV) oxide; In sodium hydroxide; under 760 Torr;

DOI:10.1016/S0040-4020(01)88647-6

Reference yield:

sorbicillin (79950-85-9) → 2',3'-dihydrosorbicillin (79950-82-6) + 2,4-dimethyl-6-hexanoyl-resorcinol (88924-67-8)

Guidance literature:

With sodium hydroxide; platinum; Hydrogenation;

DOI:10.1021/ja01192a078

upstream raw materials:

sorbicillin

1-methyl-4-nitrosobenzene

2,4-dimethylbenzene-1,3-diol

(4R*,5S*)-4,5-dibromohexanoic acid