Technology Process of 4-[ethyl(methyl)amino]benzenecarbothioamide
There total 3 articles about 4-[ethyl(methyl)amino]benzenecarbothioamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methanol; tetraphosphorus decasulfide;
at 20 ℃;
for 18h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride; water / 4 h / Reflux
2: potassium carbonate / dimethyl sulfoxide / 36 h / 60 °C / In a sealed tube
3: methanol; tetraphosphorus decasulfide / 18 h / 20 °C / Inert atmosphere
With
hydrogenchloride; methanol; tetraphosphorus decasulfide; water; potassium carbonate;
In
dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
2: hydrogenchloride; water / 4 h / Reflux
3: potassium carbonate / dimethyl sulfoxide / 36 h / 60 °C / In a sealed tube
4: methanol; tetraphosphorus decasulfide / 18 h / 20 °C / Inert atmosphere
With
hydrogenchloride; methanol; tetraphosphorus decasulfide; water; sodium hydride; potassium carbonate;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
