(2-iodo-phenyl)-octyl ether

Base Information

• Chemical Name: (2-iodo-phenyl)-octyl ether
• CAS No.: 101775-04-6
• Molecular Formula: C₁₄H₂₁IO
• Molecular Weight: 332.225
• Mol file: 101775-04-6.mol

Synonyms:(2-iodo-phenyl)-octyl ether

Chemical Property of (2-iodo-phenyl)-octyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of (2-iodo-phenyl)-octyl ether

There total 1 articles about (2-iodo-phenyl)-octyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Iodooctane (629-27-6) + 2-Iodophenol (533-58-4) → (2-iodo-phenyl)-octyl ether (101775-04-6)

Guidance literature:

With ethanol; sodium ethanolate;

DOI:10.1039/jr9590001545

Reference yield: 92.0%

(2-iodo-phenyl)-octyl ether (101775-04-6) + 1-(2-ethynylphenyl)biphenylene → 1-(2-(2-octyloxyphenylethynyl)phenyl)biphenylene

Guidance literature:

1-(2-ethynylphenyl)biphenylene; With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; at 20 ℃; for 0.5h; Inert atmosphere;

(2-iodo-phenyl)-octyl ether; With triethylamine; at 80 ℃; for 24h; Inert atmosphere;

DOI:10.1021/jacs.9b12205

Reference yield: 58.0%

methyl-d3 4-methylbenzenesulfonate (7575-93-1) + (2-iodo-phenyl)-octyl ether (101775-04-6) → C15H21(2)H3O

Guidance literature:

With manganese; chloro-trimethyl-silane; salcomine; bis(bipyridine)nickel(II) bromide; In N,N-dimethyl-formamide; at 30 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.orglett.8b01863

upstream raw materials:

1-Iodooctane

2-Iodophenol

Downstream raw materials:

(2-iodo-4-nitro-phenyl)-octyl ether

3-iodo-4-octyloxy-aniline

acetic acid-(3-iodo-4-octyloxy-anilide)