1-(Hydroxymethyl)-cycloheptanol

Base Information

• Chemical Name: 1-(Hydroxymethyl)-cycloheptanol
• CAS No.: 74397-19-6
• Molecular Formula: C8H16 O2
• Molecular Weight: 144.214
• Mol file: 74397-19-6.mol

Synonyms:1-(Hydroxymethyl)-cycloheptanol

Chemical Property of 1-(Hydroxymethyl)-cycloheptanol

Chemical Property:

• PSA: 40.46000
• LogP: 1.06400

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(Hydroxymethyl)-cycloheptanol

There total 4 articles about 1-(Hydroxymethyl)-cycloheptanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methylenecycloheptane (2505-03-5) → 1-(hydroxymethyl)cycloheptanol (74397-19-6) + cycloheptanone (502-42-1)

Guidance literature:

at 0 ℃;

Reference yield:

1-(aminomethyl)cycloheptanol (45732-95-4) → cycloactanone (502-49-8) + 1-(hydroxymethyl)cycloheptanol (74397-19-6)

Guidance literature:

With hydrogenchloride; sodium nitrite;

DOI:10.1021/ja01117a506

Reference yield:

ethyl N-methyl-N-nitrosocarbamate (615-53-2) + cycloheptanone (502-42-1) → cycloactanone (502-49-8) + 1-(hydroxymethyl)cycloheptanol (74397-19-6)

Guidance literature:

With diethyl ether; ethanol; potassium carbonate; Behandeln des Reaktionsprodukts mit wss. H₂SO₄;

DOI:10.1039/jr9390000181

upstream raw materials:

1-(aminomethyl)cycloheptanol

ethyl N-methyl-N-nitrosocarbamate

cycloheptanone

diethyl ether

Downstream raw materials:

cycloheptanecarboxaldehyde