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Hexopyranosiduronic acid, methyl 3,4-dideoxy-5-C-methyl-, methyl ester (9CI)

Base Information Edit
  • Chemical Name:Hexopyranosiduronic acid, methyl 3,4-dideoxy-5-C-methyl-, methyl ester (9CI)
  • CAS No.:791612-75-4
  • Molecular Formula:C9H16O5
  • Molecular Weight:204.223
  • Hs Code.:
  • Mol file:791612-75-4.mol
Hexopyranosiduronic acid, methyl 3,4-dideoxy-5-C-methyl-, methyl ester (9CI)

Synonyms:Hexopyranosiduronic acid, methyl 3,4-dideoxy-5-C-methyl-, methyl ester (9CI)

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Chemical Property of Hexopyranosiduronic acid, methyl 3,4-dideoxy-5-C-methyl-, methyl ester (9CI) Edit
Chemical Property:
  • PSA:64.99000 
  • LogP:0.06190 
Purity/Quality:
Safty Information:
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  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

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Technology Process of Hexopyranosiduronic acid, methyl 3,4-dideoxy-5-C-methyl-, methyl ester (9CI)

There total 1 articles about Hexopyranosiduronic acid, methyl 3,4-dideoxy-5-C-methyl-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 7 steps
1: oxalyl chloride; DMSO; Et3N / CH2Cl2 / -78 - 20 °C
2: 45 percent / BF3*OEt2 / CH2Cl2 / 18 h / 20 °C
3: LiAlH4 / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C
4: 83 percent / oxalyl chloride; DMSO; Et3N / CH2Cl2 / -78 - 20 °C
5: t-BuLi / pentane; tetrahydrofuran / 18 h / 20 °C
6: 100 percent / imidazole / dimethylformamide / 18 h / 20 °C
7: SnCl4 / CH2Cl2 / 0.5 h / 0 °C
With 1H-imidazole; lithium aluminium tetrahydride; oxalyl dichloride; boron trifluoride diethyl etherate; tert.-butyl lithium; tin(IV) chloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; pentane; 1: Swern oxidation / 4: Swern oxidation / 7: Prins-pinacol cyclization;
DOI:10.1021/ol0482745
Guidance literature:
Multi-step reaction with 8 steps
1: oxalyl chloride; DMSO; Et3N / CH2Cl2 / -78 - 20 °C
2: 45 percent / BF3*OEt2 / CH2Cl2 / 18 h / 20 °C
3: LiAlH4 / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C
4: 83 percent / oxalyl chloride; DMSO; Et3N / CH2Cl2 / -78 - 20 °C
5: t-BuLi / pentane; tetrahydrofuran / 18 h / 20 °C
6: 100 percent / imidazole / dimethylformamide / 18 h / 20 °C
7: SnCl4 / CH2Cl2 / 0.5 h / 0 °C
8: 81 percent / glacial acetic acid / 4 h / 20 °C
With 1H-imidazole; lithium aluminium tetrahydride; oxalyl dichloride; boron trifluoride diethyl etherate; tert.-butyl lithium; tin(IV) chloride; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; pentane; 1: Swern oxidation / 4: Swern oxidation / 7: Prins-pinacol cyclization;
DOI:10.1021/ol0482745
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