Technology Process of N-(2-(3-oxobutyl)phenyl)-4-methylbenzenesulfonamide
There total 7 articles about N-(2-(3-oxobutyl)phenyl)-4-methylbenzenesulfonamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl-ammonium chloride; palladium diacetate; sodium carbonate;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 48h;
DOI:10.1002/anie.201310983
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / dichloromethane / 4 h / 0 - 20 °C
2: phosphorus tribromide / dichloromethane / 1 h / 0 - 20 °C
3: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C
4: sodium hydroxide / ethanol / Reflux
With
pyridine; phosphorus tribromide; sodium hydride; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; mineral oil;
DOI:10.1039/c3cc40797g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / dichloromethane / 4 h / 0 - 20 °C
2: phosphorus tribromide / dichloromethane / 1 h / 0 - 20 °C
3: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C
4: sodium hydroxide / ethanol / Reflux
With
pyridine; phosphorus tribromide; sodium hydride; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; mineral oil;
DOI:10.1039/c3cc40797g
