Δ5,6-dehydrotriptonide

Base Information

• Chemical Name: Δ5,6-dehydrotriptonide
• CAS No.: 721883-32-5
• Molecular Formula: C₂₀H₂₀O₆
• Molecular Weight: 356.375
• Mol file: 721883-32-5.mol

Synonyms:Δ5,6-dehydrotriptonide

Chemical Property of Δ5,6-dehydrotriptonide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Δ5,6-dehydrotriptonide

There total 1 articles about Δ5,6-dehydrotriptonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

l-triptonide (38647-11-9) → Δ5,6-dehydrotriptonide (721883-32-5) + C20H21FO6

Guidance literature:

Multi-step reaction with 2 steps

1: selenium(IV) oxide / 1,4-dioxane / 24 h / Reflux; Inert atmosphere

2: dimethylaminosulphur trifluoride / dichloromethane / 1 h / 0 °C / Inert atmosphere

With selenium(IV) oxide; dimethylaminosulphur trifluoride; In 1,4-dioxane; dichloromethane;

DOI:10.1016/j.bmcl.2014.10.069

upstream raw materials:

l-triptonide

Refernces