diaquabis[4-(4H-1,2,4-triazol-4-yl)benzoato-.kappa⁽²⁾O,O']cobalt(II)

Base Information Edit

Chemical Name:diaquabis[4-(4H-1,2,4-triazol-4-yl)benzoato-.kappa⁽²⁾O,O']cobalt(II)
CAS No.:1004770-87-9
Molecular Formula:C₁₈H₁₆CoN₆O₆
Molecular Weight:471.355
Hs Code.:
Mol file:1004770-87-9.mol

diaquabis[4-(4H-1,2,4-triazol-4-yl)benzoato-.kappa<sup>(2)</sup>O,O']cobalt(II)

Synonyms:diaquabis[4-(4H-1,2,4-triazol-4-yl)benzoato-.kappa⁽²⁾O,O']cobalt(II)

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Chemical Property of diaquabis[4-(4H-1,2,4-triazol-4-yl)benzoato-.kappa⁽²⁾O,O']cobalt(II) Edit

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Technology Process of diaquabis[4-(4H-1,2,4-triazol-4-yl)benzoato-.kappa⁽²⁾O,O']cobalt(II)

There total 3 articles about diaquabis[4-(4H-1,2,4-triazol-4-yl)benzoato-.kappa⁽²⁾O,O']cobalt(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: cobalt(II) chloride hexahydrate

: 7732-18-5
water

: 157069-48-2
4-(4’-carboxyphenyl)-1,2,4-triazole

: 1004770-87-9
diaquabis[4-(4H-1,2,4-triazol-4-yl)benzoato-.kappa⁽²⁾O,O']cobalt(II)

Guidance literature:: With NEt₃; HNO₃; In water; N,N-dimethyl-formamide; High Pressure; soln. of triazole deriv. in DMF with NEt3 mixed with aq. CoCl2*6H2O at room temp.; 3 M HNO3 added, then EtOH added; soln. sealed in stainless steel reactor, heated at 85°C for 72 h; cooled to room temp.; filtered, washed with DMF and EtOH; elem. anal.;
DOI:10.1002/zaac.201000368

Reference yield: 60.0%

: 7732-18-5
water

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 157069-48-2
4-(4’-carboxyphenyl)-1,2,4-triazole

: 1004770-87-9
diaquabis[4-(4H-1,2,4-triazol-4-yl)benzoato-.kappa⁽²⁾O,O']cobalt(II)

Guidance literature:: In water; High Pressure; Co salt, acid and water in Teflon vessel placed in steel bomb; heated to413 K for 24 h; mixt. cooled slowly to room temp. over 72 h;
DOI:10.1107/S0108270107009080