α-terpinylphenylsulphide

Base Information

• Chemical Name: α-terpinylphenylsulphide
• CAS No.: 82470-87-9
• Molecular Formula: C₁₆H₂₂S
• Molecular Weight: 246.417
• Mol file: 82470-87-9.mol

Synonyms:α-terpinylphenylsulphide

Chemical Property of α-terpinylphenylsulphide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of α-terpinylphenylsulphide

There total 5 articles about α-terpinylphenylsulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-bromo-1-methoxymenth-8-yl phenylsulphide (82470-88-0) → α-terpinylphenylsulphide (82470-87-9)

Guidance literature:

With zinc; In ethanol; for 4h; Heating;

DOI:10.1016/0040-4020(82)80212-3

Reference yield:

D-limonene (5989-27-5,555-08-8,8022-90-0,9003-73-0,95327-98-3) → α-terpinylphenylsulphide (82470-87-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 71 percent / N-bromo succinimide / 1.) 0 deg C, 1 h, 2.) 19 deg C, 2 h

2: aq. perchloric acid / 1 h / 20 °C

3: 85 percent / Zn / ethanol / 4 h / Heating

With N-Bromosuccinimide; perchloric acid; zinc; In ethanol;

DOI:10.1016/0040-4020(82)80212-3

Reference yield:

thiophenol (108-98-5) → α-terpinylphenylsulphide (82470-87-9)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. perchloric acid / 1 h / 20 °C

2: 85 percent / Zn / ethanol / 4 h / Heating

With perchloric acid; zinc; In ethanol;

DOI:10.1016/0040-4020(82)80212-3

upstream raw materials:

D-limonene

thiophenol

2-bromo-1-methoxymenth-8-yl phenylsulphide

2-bromo-1-methoxy-p-menth-8-ene

Downstream raw materials:

p-menth-1-ene

(+)-Δ³-carene

4-methylisopropylbenzene

2-carene

Refernces