N-benzhydrylbenzophenone hydrazone

Base Information

• Chemical Name: N-benzhydrylbenzophenone hydrazone
• CAS No.: 25022-93-9
• Molecular Formula: C₂₆H₂₂N₂
• Molecular Weight: 362.474
• Mol file: 25022-93-9.mol

Synonyms:N-benzhydrylbenzophenone hydrazone

Chemical Property of N-benzhydrylbenzophenone hydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-benzhydrylbenzophenone hydrazone

There total 8 articles about N-benzhydrylbenzophenone hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

benzophenone azine (983-79-9) → N-benzhydrylbenzophenone hydrazone (25022-93-9)

Guidance literature:

With tetraethylammonium perchlorate; diethyl malonate; In N,N-dimethyl-formamide; at 25 ℃; electrochemical reduction;

DOI:10.1021/ja00547a007

Reference yield: 88.0%

diazodiphenylmethane (908093-98-1) → benzophenone (119-61-9) + Diphenylmethane (101-81-5) + benzophenone hydrazone (5350-57-2) + benzophenone azine (983-79-9) + N-benzhydrylbenzophenone hydrazone (25022-93-9)

Guidance literature:

With 2,2,2-trifluoroethanol; tetrabutylammonium perchlorate; In N,N-dimethyl-formamide; Product distribution; Ambient temperature; electrolytic reduction; other reagents, reagent ratio, potentials;

DOI:10.1021/ja00547a007

Reference yield: 37.0%

diazodiphenylmethane (908093-98-1) → Diphenylmethane (101-81-5) + benzophenone hydrazone (5350-57-2) + benzophenone azine (983-79-9) + N-benzhydrylbenzophenone hydrazone (25022-93-9)

Guidance literature:

With tetrabutylammonium perchlorate; diethyl malonate; In N,N-dimethyl-formamide; at 20 - 23 ℃; Mechanism; interm. anion radicals, var. temp.;

DOI:10.1039/c39800000574

upstream raw materials:

benzophenone

diphenylmethyl hydrazine

benzophenone azine

diazodiphenylmethane

Downstream raw materials:

Benzhydrylamine

N,N'-dibenzhydryl-hydrazine

Refernces

• 1、 Handoo, Kishan L.,Handoo, Sudesh K.. "Radical Anions in the Reduction of Benzophenone Azine". . p. 684 - 687. Retrieved 2007/10/02.