Technology Process of (Z)-1-(2,4-Bis-benzyloxy-3,6-dimethoxy-phenyl)-3-(2,4-bis-benzyloxy-phenyl)-propenone
There total 1 articles about (Z)-1-(2,4-Bis-benzyloxy-3,6-dimethoxy-phenyl)-3-(2,4-bis-benzyloxy-phenyl)-propenone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
ethanol;
at 40 ℃;
for 1.5h;
DOI:10.1248/cpb.46.222
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thallium (III) nitrate * 3H2O / methanol; CHCl3 / 0.5 h / 30 °C
2: 52 percent / aq. conc. HCl / acetic acid / 1 h / Ambient temperature
3: 94 percent / AlBr3 / acetonitrile / 0.67 h / 25 °C
4: 75 percent / K2CO3 / pentan-1-ol / 2 h / Heating
5: H2 / 10percent Pd/C / ethyl acetate; methanol
With
hydrogenchloride; aluminum tri-bromide; hydrogen; potassium carbonate; thallium(III) nitrate;
palladium on activated charcoal;
In
methanol; pentan-1-ol; chloroform; acetic acid; ethyl acetate; acetonitrile;
DOI:10.1248/cpb.46.222
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thallium (III) nitrate * 3H2O / methanol; CHCl3 / 0.5 h / 30 °C
2: 52 percent / aq. conc. HCl / acetic acid / 1 h / Ambient temperature
3: 94 percent / AlBr3 / acetonitrile / 0.67 h / 25 °C
4: H2 / 10percent Pd/C / ethyl acetate; methanol
With
hydrogenchloride; aluminum tri-bromide; hydrogen; thallium(III) nitrate;
palladium on activated charcoal;
In
methanol; chloroform; acetic acid; ethyl acetate; acetonitrile;
DOI:10.1248/cpb.46.222