Sodium 2,4-dinitrophenyl sulfide

Base Information

• Chemical Name: Sodium 2,4-dinitrophenyl sulfide
• CAS No.: 51256-42-9
• Molecular Formula: C₆H₃N₂O₄S*Na
• Molecular Weight: 222.157
• Mol file: 51256-42-9.mol

Synonyms:Sodium 2,4-dinitrophenyl sulfide

Chemical Property of Sodium 2,4-dinitrophenyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Sodium 2,4-dinitrophenyl sulfide

There total 2 articles about Sodium 2,4-dinitrophenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis-(2,4-dinitro-phenyl)-sulfide (2253-67-0) → Sodium 2,4-dinitrophenyl sulfide (51256-42-9)

Guidance literature:

With sodium sulfide; biphenyl; In N,N-dimethyl-formamide; at 130 ℃; for 18h;

DOI:10.1021/jo00163a013

Reference yield:

1-chloro-2,4-dinitro-benzene (97-00-7) → Sodium 2,4-dinitrophenyl sulfide (51256-42-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / Na₂S / dimethylformamide / 18 h / Heating

2: Na₂S, Biphenyl / dimethylformamide / 18 h / 130 °C

With sodium sulfide; biphenyl; In N,N-dimethyl-formamide;

DOI:10.1021/jo00163a013

Reference yield: 50.0%

ethyl bromide (74-96-4) + Sodium 2,4-dinitrophenyl sulfide (51256-42-9) → 2,4-dinitrophenyl ethyl sulfide (7343-55-7)

Guidance literature:

In N,N-dimethyl-formamide;

DOI:10.1021/jo00163a013

upstream raw materials:

bis-(2,4-dinitro-phenyl)-sulfide

1-chloro-2,4-dinitro-benzene

Downstream raw materials:

2,4-dinitrophenyl ethyl sulfide

methyl (2,4-dinitrophenylsulphanyl)ethanoate

Refernces