1-phenyl-propan-2-one phenylhydrazone

Base Information

• Chemical Name: 1-phenyl-propan-2-one phenylhydrazone
• CAS No.: 4671-23-2
• Molecular Formula: C₁₅H₁₆N₂
• Molecular Weight: 224.305
• Mol file: 4671-23-2.mol

Synonyms:1-phenyl-propan-2-one phenylhydrazone

Chemical Property of 1-phenyl-propan-2-one phenylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-phenyl-propan-2-one phenylhydrazone

There total 4 articles about 1-phenyl-propan-2-one phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-phenyl-propan-2-one semicarbazone (831-84-5) + phenylhydrazine (100-63-0) + toluene (108-88-3,15644-74-3,16713-13-6) → hydrazodicarboxamide (110-21-4) + 1-(1-methyl-2-phenyl-ethylidene)-5-phenyl carbonohydrazide + 1-phenyl-propan-2-one phenylhydrazone (4671-23-2)

Guidance literature:

at 130 - 135 ℃;

Reference yield:

propargyl benzene (10147-11-2) + phenylhydrazine (100-63-0) → 1-phenyl-propan-2-one phenylhydrazone (4671-23-2)

Guidance literature:

propargyl benzene; With triphenylcarbenium tetra(pentafluorophenyl)borate; C₄₈H₆₇NO₂Zr; In chlorobenzene; for 1h; Inert atmosphere; Glovebox;

phenylhydrazine; In chlorobenzene; at 110 ℃; for 3h; regioselective reaction; Inert atmosphere; Glovebox;

DOI:10.1039/c5dt02643a

Reference yield:

phenylhydrazine (100-63-0) + 1-phenyl-acetone (103-79-7,136675-26-8) → 1-phenyl-propan-2-one phenylhydrazone (4671-23-2)

Guidance literature:

In acetic acid;

DOI:10.1021/ol0165645

upstream raw materials:

1-phenyl-propan-2-one semicarbazone

phenylhydrazine

toluene

1-phenyl-acetone

Downstream raw materials:

2-acetamidobenzophenone

1-Benzyl-1-phenylazo-aethyl-isocyanat

1-benzyl-5-methyl-2-phenyl-1,2-dihydro-[1,2,4]triazol-3-one

5-methyl-3,6-diphenyl-3,6-dihydro-[1,3,4]oxadiazin-2-one

Refernces

• 1、 Boeckman Jr., Robert K.,Ge, Ping,Reed, Jessica E.. "New heterocyclic precursors for thermal generation of reactive, electron-rich 1,2-diaza-1,3-butadienes". . p. 3647 - 3650. Retrieved 2007/10/03.