N4,N4'-Di-m-tolyl-[1,1'-biphenyl]-4,4'-diamine

Base Information

• Chemical Name: N4,N4'-Di-m-tolyl-[1,1'-biphenyl]-4,4'-diamine
• CAS No.: 78888-06-9
• Molecular Formula: C₂₆H₂₄N₂
• Molecular Weight: 364.49
• Hs Code.: 2921590090
• DSSTox Substance ID: DTXSID10550622
• Nikkaji Number: J1.250.691K
• Wikidata: Q72446465
• Mol file: 78888-06-9.mol

Synonyms:78888-06-9;N4,N4'-Di-m-tolyl-[1,1'-biphenyl]-4,4'-diamine;3-methyl-N-[4-[4-(3-methylanilino)phenyl]phenyl]aniline;SCHEMBL513478;DTXSID10550622;N,N-Di(3-Methylphenyl)Benzidine;ONKCIMOQGCARHN-UHFFFAOYSA-N;N,N'-bis(3-methylphenyl)benzidine;AKOS015903571;SB82704;A839526;n,n'-bis(3-methylphenyl)-(1,1'biphenyl)-4,4'-diamine;N~4~,N~4'~-Bis(3-methylphenyl)[1,1'-biphenyl]-4,4'-diamine

Chemical Property of N4,N4'-Di-m-tolyl-[1,1'-biphenyl]-4,4'-diamine

Chemical Property:

• Boiling Point: 548.008oC at 760 mmHg
• Flash Point: 343.268oC
• PSA: 24.06000
• Density: 1.141g/cm3
• LogP: 7.60360
• Storage Temp.: 2-8°C
• XLogP3: 7.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 364.193948774
• Heavy Atom Count: 28
• Complexity: 405

Purity/Quality:

99% ^*data from raw suppliers

N4,N4'-Di-m-tolyl-[1,1'-biphenyl]-4,4'-diamine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=CC=C1)NC2=CC=C(C=C2)C3=CC=C(C=C3)NC4=CC=CC(=C4)C

Technology Process of N4,N4'-Di-m-tolyl-[1,1'-biphenyl]-4,4'-diamine

There total 2 articles about N4,N4'-Di-m-tolyl-[1,1'-biphenyl]-4,4'-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

4,4'-diiodobiphenyl (3001-15-8) + 1-amino-3-methylbenzene (108-44-1) → N,N'-bis(3-methylphenyl)-[1,1'-biphenyl]-4,4'-diamine (78888-06-9)

Guidance literature:

With potassium carbonate; copper; at 170 ℃; for 24h;

Reference yield:

Triphenylsilyl chloride (76-86-8) → N,N'-bis(3-methylphenyl)-[1,1'-biphenyl]-4,4'-diamine (78888-06-9)

Guidance literature:

With n-butyllithium; In hexane;

upstream raw materials:

Triphenylsilyl chloride

4,4'-diiodobiphenyl

1-amino-3-methylbenzene

Refernces

• 1、 -. "Silanamine derivative and process for the production thereof, and organical EL device using the said silanamine derivative". . . Retrieved 2008/06/13.