O-allyl-N,N'-dicyclohexyl isourea

Base Information

• Chemical Name: O-allyl-N,N'-dicyclohexyl isourea
• CAS No.: 92954-34-2
• Molecular Formula: C₁₆H₂₈N₂O
• Molecular Weight: 264.411
• Mol file: 92954-34-2.mol

Synonyms:O-allyl-N,N'-dicyclohexyl isourea

Chemical Property of O-allyl-N,N'-dicyclohexyl isourea

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O-allyl-N,N'-dicyclohexyl isourea

There total 4 articles about O-allyl-N,N'-dicyclohexyl isourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dicyclohexyl-carbodiimide (538-75-0) → O-allyl-N,N'-dicyclohexyl isourea (92954-34-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Cu₂I₂ / 20 °C

2: toluene / 15 h / 59.85 °C

With copper (I) iodide; In toluene;

DOI:10.1021/jo050392y

Reference yield:

allyl alcohol (107-18-6) + dicyclohexyl-carbodiimide (538-75-0) → O-allyl-N,N'-dicyclohexyl isourea (92954-34-2)

Guidance literature:

With copper (I) iodide; at 20 ℃;

DOI:10.1021/jo050392y

Reference yield:

allyl alcohol (107-18-6) + N,N'-dicyclohexyl-O-methyl isourea (6257-10-9) → O-allyl-N,N'-dicyclohexyl isourea (92954-34-2)

Guidance literature:

In toluene; at 59.85 ℃; for 15h;

DOI:10.1021/jo050392y

upstream raw materials:

allyl alcohol

dicyclohexyl-carbodiimide

N,N'-dicyclohexyl-O-methyl isourea

Downstream raw materials:

2-methyl-1-phenylpent-4-en-1-one

N-allylbenzamide

N,N-diallylbenzamide

N,N-Diallyltosylamide

Refernces

• 1、 Inoue, Yoshio,Toyofuku, Masanori,Taguchi, Masaaki,Okada, Shin-ichi,Hashimoto, Harukichi. "2-Allylisourea as an Effective Agent for Direct α-Allylation of Ketone and Aldehyde Assisted by Palladium(0) under Neutral Conditions". . p. 885 - 892. Retrieved 2007/10/02.