Technology Process of Methyl-(5-phenyl-[1,2,3]thiadiazol-4-yl)-carbamic acid ethyl ester
There total 4 articles about Methyl-(5-phenyl-[1,2,3]thiadiazol-4-yl)-carbamic acid ethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
ethanol;
at 40 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 92 percent / 80percent N2H4*H2O / methanol / 2 h / Ambient temperature
2: 90.5 percent / NaNO2, conc. HCl / H2O / 1 h
3: 61 percent / 1 h / Heating
4: 97 percent / K2CO3 / ethanol / 5 h / 40 °C
With
hydrogenchloride; potassium carbonate; hydrazine hydrate; sodium nitrite;
In
methanol; ethanol; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90.5 percent / NaNO2, conc. HCl / H2O / 1 h
2: 61 percent / 1 h / Heating
3: 97 percent / K2CO3 / ethanol / 5 h / 40 °C
With
hydrogenchloride; potassium carbonate; sodium nitrite;
In
ethanol; water;