Technology Process of 2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine
There total 4 articles about 2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex;
In
dichloromethane;
at 40 ℃;
for 6h;
DOI:10.1002/chem.201200499
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper; copper(II) bis(trifluoromethanesulfonate); 4,4'-di-tert-butyl-2,2'-bipyridine / benzene / 12 h / 75 °C
2.1: 9-borabicyclo[3.3.1]nonane dimer / tetrahydrofuran / 3 h / 0 - 20 °C
2.2: Pd(dppf) / 6 h / 70 °C
3.1: platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / dichloromethane / 6 h / 40 °C
With
9-borabicyclo[3.3.1]nonane dimer; platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine;
In
tetrahydrofuran; dichloromethane; benzene;
DOI:10.1002/chem.201200499
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 9-borabicyclo[3.3.1]nonane dimer / tetrahydrofuran / 3 h / 0 - 20 °C
1.2: Pd(dppf) / 6 h / 70 °C
2.1: platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / dichloromethane / 6 h / 40 °C
With
9-borabicyclo[3.3.1]nonane dimer; platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201200499