Technology Process of 4-(hydroxymethyl)-2-methoxyphenyl benzoate
There total 4 articles about 4-(hydroxymethyl)-2-methoxyphenyl benzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water;
In
dimethyl sulfoxide;
at 80 ℃;
for 14h;
Inert atmosphere;
Schlenk technique;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere
1.2: 1.5 h / 20 °C / Inert atmosphere
2.1: dmap; dicyclohexyl-carbodiimide / acetonitrile / 16 h / 20 °C / Inert atmosphere; Schlenk technique
3.1: water / dimethyl sulfoxide / 14 h / 80 °C / Inert atmosphere; Schlenk technique
With
1H-imidazole; dmap; water; dicyclohexyl-carbodiimide;
In
dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; dicyclohexyl-carbodiimide / acetonitrile / 16 h / 20 °C / Inert atmosphere; Schlenk technique
2: water / dimethyl sulfoxide / 14 h / 80 °C / Inert atmosphere; Schlenk technique
With
dmap; water; dicyclohexyl-carbodiimide;
In
dimethyl sulfoxide; acetonitrile;
