[2,4-bis(phenyl)phenyl]phenylmethanone

Base Information

• Chemical Name: [2,4-bis(phenyl)phenyl]phenylmethanone
• CAS No.: 15295-65-5
• Molecular Formula: C₂₅H₁₈O
• Molecular Weight: 334.417
• Mol file: 15295-65-5.mol

Synonyms:[2,4-bis(phenyl)phenyl]phenylmethanone

Chemical Property of [2,4-bis(phenyl)phenyl]phenylmethanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [2,4-bis(phenyl)phenyl]phenylmethanone

There total 8 articles about [2,4-bis(phenyl)phenyl]phenylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2,4-bis(trifluoromethylsulfonyloxy)benzophenone (1360171-43-2) + phenylboronic acid (98-80-6) → [2,4-bis(phenyl)phenyl]phenylmethanone (15295-65-5)

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 110 ℃; for 4h; Inert atmosphere;

DOI:10.1055/s-0031-1289649

Reference yield:

1,3-diphenylbenzene (92-06-8) → [2,4-bis(phenyl)phenyl]phenylmethanone (15295-65-5)

Guidance literature:

Multi-step reaction with 3 steps

1: bromine; carbon disulfide

2: pyridine; CuSO₄; tolunitrile / 225 °C

3: diethyl ether

With pyridine; carbon disulfide; diethyl ether; bromine; copper(II) sulfate; para-methylbenzonitrile;

DOI:10.1021/ja01165a100

Reference yield:

4’-Bromo-[1,1’:3’,1”]terphenyl (60631-83-6) → [2,4-bis(phenyl)phenyl]phenylmethanone (15295-65-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; CuSO₄; tolunitrile / 225 °C

2: diethyl ether

With pyridine; diethyl ether; copper(II) sulfate; para-methylbenzonitrile;

DOI:10.1021/ja01165a100

upstream raw materials:

2,4-diphenylbenzonitrile

1,3-diphenylbenzene

benzoyl chloride

4’-Bromo-[1,1’:3’,1”]terphenyl

Refernces