C₂₄H₃₀N₄O₄S₂

Base Information

• Chemical Name: C₂₄H₃₀N₄O₄S₂
• CAS No.: 78707-11-6
• Molecular Formula: C₂₄H₃₀N₄O₄S₂
• Molecular Weight: 502.659
• Mol file: 78707-11-6.mol

Synonyms:C₂₄H₃₀N₄O₄S₂

Chemical Property of C₂₄H₃₀N₄O₄S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C₂₄H₃₀N₄O₄S₂

There total 1 articles about C₂₄H₃₀N₄O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

butanedinitrile (110-61-2) + 1,3-diaminopropane mono-p-toluenesulfonate (59543-92-9) → C24H30N4O4S2 (78707-11-6)

Guidance literature:

at 140 ℃; for 0.5h;

DOI:10.1021/ja00404a035

Reference yield:

C24H30N4O4S2 (78707-11-6) → Spermine (71-44-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / sodium methoxide / methanol / 0.33 h / 0 °C

2: 1.) hexamethyldisilazane, fuming sulfuric acid, 2.) diisobutylaluminum hydride / 1.) reflux, 12 h, 2.) xylene, reflux, 3 d

With sulfuric acid; sodium methylate; diisobutylaluminium hydride; 1,1,1,3,3,3-hexamethyl-disilazane; In methanol;

DOI:10.1021/ja00404a035

upstream raw materials:

butanedinitrile

1,3-diaminopropane mono-p-toluenesulfonate

Downstream raw materials:

Spermine