2-iodo-1-phenylethyl 2-butynoate

Base Information

• Chemical Name: 2-iodo-1-phenylethyl 2-butynoate
• CAS No.: 115377-04-3
• Molecular Formula: C₁₂H₁₁IO₂
• Molecular Weight: 314.123
• Mol file: 115377-04-3.mol

Synonyms:2-iodo-1-phenylethyl 2-butynoate

Chemical Property of 2-iodo-1-phenylethyl 2-butynoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-iodo-1-phenylethyl 2-butynoate

There total 1 articles about 2-iodo-1-phenylethyl 2-butynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 2-Butynoic acid (590-93-2) → 2-iodo-1-phenylethyl 2-butynoate (115377-04-3)

Guidance literature:

With N-iodo-succinimide; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1016/S0040-4020(01)85740-9

Reference yield: 77.0%

2-iodo-1-phenylethyl 2-butynoate (115377-04-3) → (3E)-dihydro-3-(iodoethylidene)-5-phenyl-2(3H)-furanone (115377-13-4)

Guidance literature:

With dibenzoyl peroxide; In benzene; for 14h; Heating;

DOI:10.1016/S0040-4020(01)85740-9

upstream raw materials:

styrene

2-Butynoic acid

Downstream raw materials:

(3E)-dihydro-3-(iodoethylidene)-5-phenyl-2(3H)-furanone

Refernces

• 1、 Haaima,Lynch,Routledge,Weavers. "Synthesis of iodoalkylidene lactones from alkenes". . p. 4229 - 4252. Retrieved 2007/10/02.