ethyl p-methoxybenzyl sulfide

Base Information

• Chemical Name: ethyl p-methoxybenzyl sulfide
• CAS No.: 83318-92-7
• Molecular Formula: C₁₀H₁₄OS
• Molecular Weight: 182.287
• Mol file: 83318-92-7.mol

Synonyms:ethyl p-methoxybenzyl sulfide

Chemical Property of ethyl p-methoxybenzyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl p-methoxybenzyl sulfide

There total 21 articles about ethyl p-methoxybenzyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C50H54O8 → 1,2,5,6-tetra-O-benzyl-D-mannitol (20196-69-4) + ethyl p-methoxybenzyl sulfide (83318-92-7)

Guidance literature:

With aluminium trichloride; ethanethiol; In dichloromethane; for 1.5h; Ambient temperature;

DOI:10.1055/s-1997-990

Reference yield: 93.0%

1-((benzyloxy)methyl)-4-methoxybenzene (3613-53-4) → ethyl p-methoxybenzyl sulfide (83318-92-7) + benzyl alcohol (100-51-6,185532-71-2)

Guidance literature:

With aluminium trichloride; ethanethiol; In dichloromethane; for 0.5h; Ambient temperature;

DOI:10.1055/s-1997-990

Reference yield: 93.0%

1-((benzyloxy)methyl)-4-methoxybenzene (3613-53-4) + ethanethiol (75-08-1) → ethyl p-methoxybenzyl sulfide (83318-92-7) + benzyl alcohol (100-51-6,185532-71-2)

Guidance literature:

With aluminium trichloride; In dichloromethane; for 0.5h; Mechanism; Ambient temperature; Lewis acid-catalyzed deprotection of various p-methoxybenzyl ethers;

DOI:10.1055/s-1997-990

upstream raw materials:

1-(4-Methoxy-benzyl)-2-methylsulfanyl-4,6-diphenyl-pyridinium; iodide

sodium thioethylate

1-((benzyloxy)methyl)-4-methoxybenzene

1-methoxy-4-((4-nitrophenoxy)methyl)benzene

Downstream raw materials:

1-ethanesulfonylmethyl-4-methoxy-benzene

4-methoxy-benzaldehyde

Refernces

• 1、 Zhao, Guangkuan,Yuan, Ling-Zhi,Alami, Mouad,Provot, Olivier. "Chlorotrimethylsilane and Sodium Iodide: A Remarkable Metal-Free Association for the Desulfurization of Benzylic Dithioketals under Mild Conditions". . p. 2522 - 2536. Retrieved 2018/05/14.
• 2、 Ikeshita, Kei-ichiro,Kihara, Nobuhiro,Sonoda, Motohiro,Ogawa, Akiya. "Lewis acid-catalyzed reduction of dithioacetals by 1,4-cyclohexadiene". . p. 3025 - 3028. Retrieved 2008/02/06.