diethyl 5-methylisophthalate

Base Information Edit

Chemical Name:diethyl 5-methylisophthalate
CAS No.:100613-06-7
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:
Mol file:100613-06-7.mol

Synonyms:diethyl 5-methylisophthalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 5-methylisophthalate Edit

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Technology Process of diethyl 5-methylisophthalate

There total 4 articles about diethyl 5-methylisophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 100613-06-7
diethyl 5-methylisophthalate

Guidance literature:: With thionyl chloride; at 20 ℃; for 3h; Cooling with ice;

Reference yield: 82.0%

: 64-17-5
ethanol

: 499-49-0
5-methylisophthalic aicd

: 100613-06-7
diethyl 5-methylisophthalate

Guidance literature:: With hydrogenchloride; for 2h;
DOI:10.1021/ja00093a026

Reference yield:

: 108-67-8
1,3,5-trimethyl-benzene

: 100613-06-7
diethyl 5-methylisophthalate

Guidance literature:: Multi-step reaction with 3 steps

1: diluted nitric acid / man loest die ausgeschiedenen Saeuren in Soda, faellt mit Salzsaeure und destilliert mit Wasser, wobei Uvitinsaeure zurueckbleibt

2: K₂cr2O₇; diluted sulfuric acid

3: HCl

With hydrogenchloride; potassium dichromate; sulfuric acid; nitric acid;