di-2-thienyl ketone 2,4-dinitrophenyl hydrazone

Base Information

• Chemical Name: di-2-thienyl ketone 2,4-dinitrophenyl hydrazone
• CAS No.: 109407-70-7
• Molecular Formula: C₁₅H₁₀N₄O₄S₂
• Molecular Weight: 374.401
• Mol file: 109407-70-7.mol

Synonyms:di-2-thienyl ketone 2,4-dinitrophenyl hydrazone

Chemical Property of di-2-thienyl ketone 2,4-dinitrophenyl hydrazone

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of di-2-thienyl ketone 2,4-dinitrophenyl hydrazone

There total 2 articles about di-2-thienyl ketone 2,4-dinitrophenyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

di(thiophen-2-yl)methanone (704-38-1) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → di-2-thienyl ketone 2,4-dinitrophenyl hydrazone (109407-70-7)

Guidance literature:

With hydrogenchloride; In ethanol; for 5h; Reflux;

DOI:10.1016/j.molstruc.2018.07.008

Reference yield:

1,1,1-trichloro-2,2-di-[2]thienyl-ethane (6345-58-0) → di-2-thienyl ketone 2,4-dinitrophenyl hydrazone (109407-70-7)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanolic KOH-solution / Erhitzen des Reaktionsprodukts mit Chrom(VI)-oxid in Essigsaeure

With potassium hydroxide;

DOI:10.1021/ja01203a003

upstream raw materials:

di(thiophen-2-yl)methanone

(2,4-dinitro-phenyl)-hydrazine

1,1,1-trichloro-2,2-di-[2]thienyl-ethane

Refernces