hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane

Base Information

• Chemical Name: hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane
• CAS No.: 17955-48-5
• Molecular Formula: C₁₅H₃₆Si₂
• Molecular Weight: 272.622
• Mol file: 17955-48-5.mol

Synonyms:hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane

Chemical Property of hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane

There total 5 articles about hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

3,3,3-trichloro-1-propene (2233-00-3) → 1,1,1-trichloropropane (7789-89-1) + 1,1-dichloropropene (563-58-6) + 3,3,3-trichloropropyltriethylsilane (17873-97-1) + hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane (17955-48-5)

Guidance literature:

With triethylsilane; dihydrogen hexachloroplatinate; isopropyl alcohol; at 20 ℃; for 48h; Further byproducts given;

DOI:10.1007/BF00956356

Reference yield: 55.0%

triethylsilane (617-86-7) + 3,3,3-trichloro-1-propene (2233-00-3) → 1,1,1-trichloropropane (7789-89-1) + 1,1-dichloropropene (563-58-6) + 3,3,3-trichloropropyltriethylsilane (17873-97-1) + hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane (17955-48-5)

Guidance literature:

With dihydrogen hexachloroplatinate; isopropyl alcohol; at 20 ℃; for 48h; Further byproducts given. Title compound not separated from byproducts;

DOI:10.1007/BF00956356

Reference yield: 55.0%

triethylsilane (617-86-7) + 3,3,3-trichloro-1-propene (2233-00-3) → 1,1-dichloropropene (563-58-6) + 3,3,3-trichloropropyltriethylsilane (17873-97-1) + hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane (17955-48-5) + ((E)-1-Chloro-propenyl)-triethyl-silane (114700-65-1)

Guidance literature:

With dihydrogen hexachloroplatinate; isopropyl alcohol; at 20 ℃; for 48h; Further byproducts given. Title compound not separated from byproducts;

DOI:10.1007/BF00956356

upstream raw materials:

triethylsilane

3,3,3-trichloro-1-propene

allyl-trimethyl-silane

Refernces

• 1、 Galkina, M. A.,Chukovskaya, E. Ts.,Freidlina, R. Kh.. "HYDROSILATION OF α,α,α-TRICHLOROALKENES IN THE PRESENCE OF H2PtCl6-6H2O". . p. 1010 - 1012. Retrieved 2007/10/02.