1-Butyl-4-methylpyridinium bromide

Base Information

• Chemical Name: 1-Butyl-4-methylpyridinium bromide
• CAS No.: 65350-59-6
• Molecular Formula: C10H16 N . Br
• Molecular Weight: 230.148
• Hs Code.: 2933399090
• European Community (EC) Number: 626-907-7
• ChEMBL ID: CHEMBL3182875
• DSSTox Substance ID: DTXSID2049345
• Mol file: 65350-59-6.mol

Synonyms:1-Butyl-4-methylpyridinium bromide;65350-59-6;1-butyl-4-methylpyridin-1-ium bromide;1-butyl-4-methylpyridin-1-ium;bromide;DTXSID2049345;N-butyl-4-metylpyridinium bromide;SCHEMBL193632;CHEMBL3182875;DTXCID9029302;N-butyl-4-methylpyridinium bromide;1-butyl-4-methyl pyridinium bromide;Tox21_202683;MFCD06798209;AKOS015833018;CS-W012963;1-butyl-4-methyl-pyridin-1-ium bromide;NCGC00260231-01;AS-10289;CAS-65350-59-6;B2700;A51103;A835078;Pyridinium,1-butyl-4-methyl-, bromide (1:1);1-butyl-4-methylpyridin-1-ium,bromide;1-Butyl-4-methylpyridinium Bromide

Chemical Property of 1-Butyl-4-methylpyridinium bromide

Chemical Property:

• Melting Point: 134-136 °C
• PSA: 3.88000
• LogP: -0.91340
• Storage Temp.: Inert atmosphere,Room Temperature
• Water Solubility.: Soluble in water
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 229.04661
• Heavy Atom Count: 12
• Complexity: 93

Purity/Quality:

98% ^*data from raw suppliers

1-Butyl-4-methylpyridin-1-iumBromide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC[N+]1=CC=C(C=C1)C.[Br-]

Technology Process of 1-Butyl-4-methylpyridinium bromide

There total 2 articles about 1-Butyl-4-methylpyridinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

picoline (108-89-4) + 1-bromo-butane (109-65-9) → N-butyl-4-methylpyridinium bromide (65350-59-6)

Guidance literature:

Darkness;

DOI:10.1016/j.molliq.2015.05.028

Reference yield:

1-n-butyl-4-methylpyridinium-p-toluenesulphonate (880143-38-4) → N-butyl-4-methylpyridinium bromide (65350-59-6)

Guidance literature:

With hydrogen bromide; In water;

DOI:10.14233/ajchem.2018.21086

Reference yield: 100.0%

sodium salicylate (54-21-7) + N-butyl-4-methylpyridinium bromide (65350-59-6) → 1-butyl-4-methylpyridinium salicylate (1609103-04-9)

Guidance literature:

In acetone; for 72h;

DOI:10.1002/chem.201301363

upstream raw materials:

picoline

1-bromo-butane

1-n-butyl-4-methylpyridinium-p-toluenesulphonate

Downstream raw materials:

6-methylazulene

methyl bromide

4-(4-aminostyryl)-1-butylpyridinium bromide

1-butyl-4-methylpyridinium salicylate

Refernces

• 1、 Balapanuru, Janardhan,Yang, Jia-Xiang,Xiao, Si,Bao, Qiaoliang,Jahan, Maryam,Polavarapu, Lakshminarayana,Wei, Ji,Xu, Qing-Hua,Loh, Kian Ping. "A graphene oxide-organic dye ionic complex with DNA-sensing and optical-limiting properties". . p. 6549 - 6553. Retrieved 2010.
• 2、 Babu, Balaji,Mack, John,Magadla, Aviwe,Nyokong, Tebello. "Positively charged styryl pyridine substituted Zn(ii) phthalocyanines for photodynamic therapy and photoantimicrobial chemotherapy: Effect of the number of charges". supporting information. p. 9129 - 9136. Retrieved 2021/07/14.
• 3、 Maeng, Chanyoung,Son, Jeong-Yu,Lee, Seung Cheol,Baek, Yonghyeon,Um, Kyusik,Han, Sang Hoon,Ko, Gi Hoon,Han, Gi Uk,Lee, Kyungsup,Lee, Kooyeon,Lee, Phil Ho. "Expansion of Azulenes as Nonbenzenoid Aromatic Compounds for C-H Activation: Rhodium- And Iridium-Catalyzed Oxidative Cyclization of Azulene Carboxylic Acids with Alkynes for the Synthesis of Azulenolactones and Benzoazulenes". supporting information. p. 3824 - 3837. Retrieved 2020/02/28.