Technology Process of C22H28O6S
There total 3 articles about C22H28O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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99297-03-7
Toluene-4-sulfonic acid (3S,3aS,5aR,6R,9bS)-3,5a,9-trimethyl-2-oxo-2,3,3a,4,5,5a,6,7,8,9b-decahydro-naphtho[1,2-b]furan-6-yl ester
- Guidance literature:
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With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
for 14h;
Ambient temperature;
DOI:10.1021/jo00350a081
- Guidance literature:
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Multi-step reaction with 2 steps
1: 90 percent / pyridine / 20 h / Ambient temperature
2: 89.7 percent / MCPBA / CH2Cl2 / 14 h / Ambient temperature
With
pyridine; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
DOI:10.1021/jo00350a081
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 83 percent / NaBH4 / ethanol / 2.5 h / Ambient temperature
2: 90 percent / pyridine / 20 h / Ambient temperature
3: 89.7 percent / MCPBA / CH2Cl2 / 14 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid;
In
ethanol; dichloromethane;
DOI:10.1021/jo00350a081