Technology Process of Phosphinous acid, diphenyl-, anhydride with diethylborinic acid
There total 2 articles about Phosphinous acid, diphenyl-, anhydride with diethylborinic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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diethylboryl-pivalate;
byproducts: C2H6; heating to 100°C for 30 min under exclusion of air and moisture; evapn. of the excess of triethylborane in vacuo, elem. anal.;
- Guidance literature:
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diethylboryl-pivalate;
byproducts: C2H6; heating of the phosphine oxide and 2 mol diborane to 100°C for 30 min under exclusion of air and moisture; evapn. of the excess of triethylborane in vacuo, elem. anal.;
- Guidance literature:
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In
toluene;
heating at 120°C for 30 min under exclusion of air and moisture; monitored by NMR;
