Ethanethioamide, N-methyl-N-(4-nitrophenyl)-

Base Information

• Chemical Name: Ethanethioamide, N-methyl-N-(4-nitrophenyl)-
• CAS No.: 65052-84-8
• Molecular Formula: C9H10 N2 O2 S
• Molecular Weight: 210.25
• Hs Code.: 2930909090
• Mol file: 65052-84-8.mol

Synonyms:Ethanethioamide, N-methyl-N-(4-nitrophenyl)-

Chemical Property of Ethanethioamide, N-methyl-N-(4-nitrophenyl)-

Chemical Property:

• Boiling Point: 336.7±44.0 °C(Predicted)
• PKA: -5.08±0.50(Predicted)
• PSA: 81.15000
• Density: 1.307±0.06 g/cm3(Predicted)
• LogP: 2.90150

Purity/Quality:

99% ^*data from raw suppliers

ETHANETHIOAMIDE, N-METHYL-N-(4-NITROPHENYL)- 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanethioamide, N-methyl-N-(4-nitrophenyl)-

There total 2 articles about Ethanethioamide, N-methyl-N-(4-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

N-methyl-4-nitroacetanilide (121-95-9) → N-Methyl-4-nitro-thioacetanilid (65052-84-8)

Guidance literature:

With Lawessons reagent; In toluene; at 100 - 110 ℃; for 2h; Inert atmosphere;

DOI:10.1021/acs.joc.1c00801

Reference yield:

→ N-Methyl-4-nitro-thioacetanilid (65052-84-8)

Guidance literature:

durch Schwefelung von N-Methyl-4-nitroacetanilid mit P4S10 in Pyridin;

upstream raw materials:

N-methyl-4-nitroacetanilide

Refernces