Artanin

Base Information

• Chemical Name: Artanin
• CAS No.: 96917-26-9
• Molecular Formula: C₁₆H₁₈O₅
• Molecular Weight: 290.316
• Mol file: 96917-26-9.mol

Synonyms:2H-1-Benzopyran-2-one,5,7-dimethoxy-8-[(3-methyl-2-butenyl)oxy]- (9CI); Artanin

Chemical Property of Artanin

Chemical Property:

• Melting Point: 104-107 °C(Solv: ethyl ether (60-29-7); hexane (110-54-3))
• Boiling Point: 460.5±45.0 °C(Predicted)
• PSA: 57.90000
• Density: 1.168±0.06 g/cm3(Predicted)
• LogP: 3.15520

Purity/Quality:

98%Min ^*data from raw suppliers

Artanin ≥98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Artanin

There total 2 articles about Artanin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

8-hydroxy-5,7-dimethoxycoumarin (leptodactylone) (61899-44-3) + 1-Bromo-3-methyl-butene (16416-41-4) → artanin (96917-26-9)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1016/j.tet.2008.02.059

Reference yield: 98.0%

8-hydroxy-5,7-dimethoxycoumarin (leptodactylone) (61899-44-3) + prenyl bromide (870-63-3) → artanin (96917-26-9)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1016/j.bmc.2009.08.002

upstream raw materials:

8-hydroxy-5,7-dimethoxycoumarin (leptodactylone)

1-Bromo-3-methyl-butene

prenyl bromide

Refernces

• 1、 Maes, Dominick,Riveiro, Maria Eugenia,Shayo, Carina,Davio, Carlos,Debenedetti, Silvia,De Kimpe, Norbert. "Total synthesis of naturally occurring 5,6,7- and 5,7,8-trioxygenated coumarins". . p. 4438 - 4443. Retrieved 2008/09/21.