C₃₉H₆₂O₁₇

Base Information

• Chemical Name: C₃₉H₆₂O₁₇
• CAS No.: 1338602-92-8
• Molecular Formula: C₃₉H₆₂O₁₇
• Molecular Weight: 802.911
• Mol file: 1338602-92-8.mol

Synonyms:C₃₉H₆₂O₁₇

Chemical Property of C₃₉H₆₂O₁₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₉H₆₂O₁₇

There total 6 articles about C₃₉H₆₂O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

C33H57ClO15 + hydroquinone (123-31-9,8027-02-9) → C39H62O17 (1338602-92-8)

Guidance literature:

hydroquinone; With triethylamine; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

C₃₃H₅₇ClO₁₅; In tetrahydrofuran; at 20 ℃; for 10h; Inert atmosphere;

DOI:10.5012/bkcs.2011.32.7.2193

Reference yield:

C34H60O16 (1338602-87-1) → C39H62O17 (1338602-92-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium hydroxide / methanol; water / 4 h / Inert atmosphere; Reflux

1.2: Inert atmosphere; Reflux

2.1: thionyl chloride; N,N-dimethyl-formamide / chloroform / 4 h / 20 °C / Inert atmosphere; Cooling with ice

3.1: triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.2: 10 h / 20 °C / Inert atmosphere

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; potassium hydroxide; In tetrahydrofuran; methanol; chloroform; water;

DOI:10.5012/bkcs.2011.32.7.2193

Reference yield:

triethylene glucol monomethyl ether (112-35-6,95507-80-5) → C39H62O17 (1338602-92-8)

Guidance literature:

Multi-step reaction with 7 steps

1.1: dichloromethane / 10 h / 20 °C / Inert atmosphere

2.1: sodium / 49 h / 50 - 100 °C / Inert atmosphere

3.1: dichloromethane / 10 h / 20 °C / Inert atmosphere

4.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 60 °C / Inert atmosphere

5.1: potassium hydroxide / methanol; water / 4 h / Inert atmosphere; Reflux

5.2: Inert atmosphere; Reflux

6.1: thionyl chloride; N,N-dimethyl-formamide / chloroform / 4 h / 20 °C / Inert atmosphere; Cooling with ice

7.1: triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

7.2: 10 h / 20 °C / Inert atmosphere

With thionyl chloride; sodium; potassium carbonate; triethylamine; N,N-dimethyl-formamide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;

DOI:10.5012/bkcs.2011.32.7.2193

upstream raw materials:

hydroquinone

C₃₄H₆₀O₁₆

C₃₃H₅₈O₁₆

triethylene glucol monomethyl ether

Downstream raw materials:

C₄₃H₆₄N₂O₁₈

Refernces