9-phenyl-10-methylacridinyl radical

Base Information

• Chemical Name: 9-phenyl-10-methylacridinyl radical
• CAS No.: 100667-92-3
• Molecular Formula: C₂₀H₁₆N
• Molecular Weight: 270.354
• Mol file: 100667-92-3.mol

Synonyms:9-phenyl-10-methylacridinyl radical

Chemical Property of 9-phenyl-10-methylacridinyl radical

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-phenyl-10-methylacridinyl radical

There total 19 articles about 9-phenyl-10-methylacridinyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

10-methyl-9-phenylacridinium trifluoromethanesulphonate (94707-38-7) → 9-phenyl-10-methylacridinyl radical (100667-92-3)

Guidance literature:

With PPN⁽¹⁺⁾*Re(CO)5^(1-); In tetrahydrofuran; at 20 ℃;

DOI:10.1002/(SICI)1099-1395(199707)10:7<542::AID-POC918>3.0.CO;2-O

Reference yield:

10-methyl-9-phenylacridin-10-ium perchlorate → 9-phenyl-10-methylacridinyl radical (100667-92-3)

Guidance literature:

With tetramethysemiquinone radical anion; In acetonitrile; at 298 ℃; Further Variations:; Solvents; Temperatures; Kinetics;

DOI:10.1021/ja004311l

Reference yield:

10-Methyl-9-phenyl-9,10-dihydro-acridine → 9-phenyl-10-methylacridinyl radical (100667-92-3)

Guidance literature:

In acetonitrile; at 24.84 ℃; Kinetics;

DOI:10.1021/ja9941375

upstream raw materials:

N-methyl-9-phenylacridinium cation

10-methyl-9-phenylacridin-10-ium chloride

piperidine

pyridine

Refernces

• 1、 Fukuzumi,Ohkubo,Suenobu,Kato,Fujitsuka,Ito. "Photoalkylation of 10-alkylacridinium ion via a charge-shift type of photoinduced electron transfer controlled by solvent polarity". . p. 8459 - 8467. Retrieved 2001.
• 2、 Anne, Agnès,Fraoua, Sylvie,Hapiot, Philippe,Moiroux, Jacques,Savéant, Jean-Michel. "Steric and kinetic isotope effects in the deprotonation of cation radicals of NADH synthetic analogues". . p. 7412 - 7421. Retrieved 2007/10/02.